The Effect of the Ball Size on the Product Characteristics of Shaker HEBM to Produce Nano Particle from Bamboo Charcoal

Supriyono Sastrowiyono

doi:10.22219/jemmme.v3i1.5761

Authors

Supriyono Sastrowiyono University of Muhammadiyah Surakarta

DOI:

https://doi.org/10.22219/jemmme.v3i1.5761

Abstract

The objective of this research is to study the effect of ball size on characteristics of product of shaker high energy ball milling (HEBM) to produce nano particle from bamboo charcoal. A new shaker mechanism is developed. The characteristics of the particle are represented by particle size, surface morphology, and the substances presence in the product. Particle size analyzer (PSA) is conducted to have the particle sizes, whereas SEM and EDX are used to have surface morphology and substances presence in the products respectively. The mixtures of 11 gr of bamboo charcoal powder of 200 meshes and about 299 gr of steel ball are placed in vials. The vial is from stainless steel cylinder with 1 inch diameter and 120 mm length. The stroke of the shaker is 54 mm at increasing speed of connecting rod pulley for every 1 million cycles. The total number of cycle is 3 million. Therefore, the connecting rod speed of the first 1 million cycles is 300 rpm, the second is 333 rpm, and the third is 367 rpm. The steel ball sizes are and inch. PSA results indicate that there is no certain correlation between the steel ball size and particle size. The final shape of the particles is determined by fracture mechanism. The highest substance presence in the result is carbon and followed by silicon.

Downloads

Download data is not yet available.

References

K. V Nagesha, M. Rajanish, and D. Shivappa, “A Review On Mechanical Alloying,” Int. J. Eng. Res. Appl., vol. 3, no. 3, pp. 921–924, 2013.

H. F. Li and R. V. Ramanujan, “Microstructural Evolution and Nanocrystalline Formation Kinetics in FeCo Based Alloys During Mechanical Alloying,” J. Metastable Nanocrystalline Mater., vol. 23, pp. 187–190, 2005.

S. R. Mishra et al., “Magnetic properties of iron nitride-alumina nanocomposite materials prepared by high-energy ball milling,” Eur. Phys. J. D - At. Mol. Opt. Phys., vol. 24, no. 1–3, pp. 93–96, 2003.

R. Hamzaoui, S. Guessasma, and O. ElKedim, “Analysis of structure and magnetic properties of nanocrystalline milled alloys,” J. Alloys Compd., vol. 462, no. 1–2, pp. 29–37, 2008.

A. P. W. Pilarczyk, R. Nowosielski, “Structure and properties of Fe-Co-Ni-B-Si-Nb alloy prepared by mechanical alloying method,” J. Achiev. Mater. Manuf. Eng., vol. 30, no. 2, 2008.

M. El-Eskandarany, K. Aoki, and K. Sumiyama, “Cyclic phase transformations of mechanically alloyed Co 75 Ti 25 powders,” Acta, vol. 50, pp. 1113–1123, 2002.

Y. C. Ã, C. P. Li, H. Chen, and Y. Chen, “One-dimensional nanomaterials synthesized using high-energy ball milling and annealing process,” Sci. Technol. Adv. Mater., vol. 7, no. 2006, pp. 839–846, 2007.

H. Sa’diyah, S. Nurhimawan, S. A. Fatoni, Irmansyah, and Irzaman, “Ektraksi silikon dioksida dari daun bambu,” Pros. Semin. Nas. Fiz., vol. V, no. Oktober, pp. 13–16, 2016.

R. Ikono et al., “SINTESIS NANOPARTIKEL ZnO DENGAN METODE MECHANOCHEMICAL MILLING,” pp. 60–62, 2012.

J. W. Yan, Y. Liu, A. F. Peng, and Q. G. Lu, “Fabrication of nano-crystalline W-Ni-Fe pre-alloyed powders by mechanical alloying technique,” Trans. Nonferrous Met. Soc. China (English Ed., vol. 19, no. SUPPL. 3, pp. s711–s717, 2009.

Y. Do, J. Youl, J. Kim, and H. Jeon, “Formation of nanocrystalline Fe – Co powders produced by mechanical alloying,” Mater. Sci. Eng., vol. 291, pp. 17–21, 2000.

J. Eckert and I. Bo, “Nanostructure formation and properties of ball-milled NiAl intermetallic compound,” Mater. Sci. Eng., vol. 240, pp. 619–624, 1997.

M. Umemoto, Z. G. Liu, K. Masuyama, X. J. Hao, and K. Tsuchiya, “Nanostructured Fe-C Alloys Produced by Ball Milling,” Scr. Mater., vol. 44, pp. 1741–1745, 2001.